About this product
2,3,4,6-O-????-D-???,
2,3,4,6-Tetra-O-acetyl-beta-D-glucopyranose is a synthetic compound that is used as an oral medicine. It has been shown to be effective in the treatment of arthritis and other inflammatory conditions. The preparation process involves the conversion of 2,3,4,6-tetra-O-acetyl-beta-D-glucopyranose into besifloxacin and chiral 2,3,4,6 tetra acetyl beta D glucopyranose. This drug is then recrystallized with potassium carbonate to produce besifloxacin as a white crystalline solid. Recrystallizing this drug produces besifloxacin as a white crystalline solid. 2,3,4,6 Tetra O Acetyl Beta D Glucopyranose can be detected using analytical chemistry methods such as reversed phase liquid.
CAS Number 3947-62-4
Product Name 2,3,4,6-Tetra-O-acetyl-beta-D-glucose
IUPAC Name [(2R,3R,4S,5R,6R)-3,4,5-triacetyloxy-6-hydroxyoxan-2-yl]methyl acetate
Molecular Formula C14H20O10
Molecular Weight 348.303 g/mol
InChI InChI=1S/C14H20O10/c1-6(15)20-5-10-11(21-7(2)16)12(22-8(3)17)13(14(19)24-10)23-9(4)18/h10-14,19H,5H2,1-4H3/t10-,11-,12+,13-,14-/m1/s1
InChI Key IEOLRPPTIGNUNP-RKQHYHRCSA-N
SMILES CC(=O)OCC1C(C(C(C(O1)O)OC(=O)C)OC(=O)C)OC(=O)C
Canonical SMILES CC(=O)OCC1C(C(C(C(O1)O)OC(=O)C)OC(=O)C)OC(=O)C
Isomeric SMILES CC(=O)OC[C@@H]1[C@H]([C@@H]([C@H]([C@@H](O1)O)OC(=O)C)OC(=O)C)OC(=O)C
CAS No: 3947-62-4,10343-06-3 Synonyms: 2,3,4,6-Tetraacetate D-glucopyranose MDL No: MFCD00061634 Chemical Formula: C14H20O10 Molecular Weight: 348.303
COA:
Product name : 2,3,4,6-Tetra-O-acetyl-beta-D-glucopyranose
CAS : 3947-62-4 M .F. : C 14 H 20 O 10 M .W. : 348.303 Batch No : 20130314 Quantity :375g
Items
Standards
Results
Appearance
White crystalline powder
Positive
Solubility
Readily soluble in CHC 3 and
insoluble in water
Positive
NMR and MS
Should comply
Complies
Identification
IR and TLC
Positive
M.P.
120 ? ?125 ?
122 ? ?124 ?
Specific rotation
[?]20/D ? (C = 1 ? in CHC 3 )
+30? to +32?
+31.4?
Loss Weight On Dryness
Max. 0.5%
Complies
TLC
One spot
Complies
Residue On Ignition
Max. 0.5%
Complies
Assay (HPLC)
Min. 98%
98.5%
References:
1. Sambaiaha T, Fanwick PE, Cushman M, Synthesis 2001, p1450-1452
2. Sofian A, Lee C, J. Carbohydr. Chem. 2001, Vol20, Pt6, p431-440